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In this report, the synthesis of iron borides has been studied. Iron and boron powders have been mixed in amounts corresponding to 50 at-% of each element. Differential scanning calorimetry (DSC) has been used to observe any reactions taking place up to a temperature of 1550 °C at heating rates of 5, 10 and 10 K/min, both for pre-compacted Fe-B powder mixtures as well as loose powders. The results
