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This master thesis consists of two parts, which both deal with NMR studies of the carbohydrate-binding domain of the protein galectin-3 (Gal3C). In the first part, 19F relaxation of two difluorinated diastereomeric ligands bound to Gal3C was analyzed with the model-free approach to extract information about the dynamics. The second part reports the assignments of the backbone amide 1H/15N resonanc
